Reaction #1265362

ord-91b02176b78b49d5b52c0f8a167644b2

Reaction equation

OCCN1CCOCC1
2-morpholinoethanol
O=C(Cl)c1cccc2ccccc12
1-naphthoyl chloride
O=C(OCCN1CCOCC1)c1cccc2ccccc12
2-morpholinoethyl 1-naphthalenecarboxylate
Yield 94.0%

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThe procedure of Synthesis Example 1

Procedure

The procedure of Synthesis Example 1 was repeated except that 2-morpholinoethanol was used instead of the triethanolamine, and 1-naphthoyl chloride was used instead of the benzoyl chloride, to give 2-morpholinoethyl 1-naphthalenecarboxylate in a yield of 94%.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07276324B2uspto-grants-2007_10