Reaction #1254222

Reaction equation

N-butyl-N-cyclooctylpyrrolidinium iodide salt

hydroxide

→

N-butyl-N-cyclooctylpyrrolidinium hydroxide

Solvents

water

Conditions

Workup

1. 1
   workup.ADDITIONof Ion Exchange Resin OH (BIO RAD® AG1-X8) is added
2. 2
   FiltrationThe mixture is filtered
3. 3
   Washthe solids rinsed with an additional 250 ml
4. 4
   FiltrationThe original mixture is filtered

Procedure

N-butyl-N-cyclooctylpyrrolidinium iodide salt (95 gms., 0.26 mole) is dissolved in 300 ml. water in a 1000 ml. plastic bottle. To the solution, 300 gms. of Ion Exchange Resin OH (BIO RAD® AG1-X8) is added and the mixture is stirred at room temperature overnight. The mixture is filtered and the solids rinsed with an additional 250 ml. of water. The original mixture is filtered and the rinses are combined and a small amount is titrated with 0.1N HCl to indicate the presence of 0.24 mol hydroxide (0.24 mol N-butyl-N-cyclooctylpyrrolidinium hydroxide) in the solution.

Source