Reaction #1234

ord-7949d567ab7542a8990b7bcf17a467de

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Following the basic procedure of Example 7(f), by reacting 2.8 g (10 mmol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthrylboronic acid with 1.84 g (6.7 mmol) of methyl 3-methyl-4-iodobenzoate, 1.37 g (53%) of methyl 3-methyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)benzoate was obtained in the form of a yellow oil.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05723499uspto-grants-1998_03