Reaction #1056

ord-04e4aa0d550f42b3965842045af58c87

Reaction equation

c1ccc2c(c1)NCCCO2
2,3,4,5-tetrahydro-1,5-benzoxazepine
O=C(Cl)CCCCl
4-chlorobutyryl chloride
O=C(CCCCl)N1CCCOc2ccccc21
5-(4-chlorobutyryl)-2,3,4,5-tetrahydro-1,5-benzoxazepine

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    Otherto produce the above compound in the same way as Reference Example 8

Procedure

2,3,4,5-tetrahydro-1,5-benzoxazepine and 4-chlorobutyryl chloride were used to produce the above compound in the same way as Reference Example 8.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05723475uspto-grants-1998_03