Reaction #1050

ord-b9bc34feae494fc2941a6a9edafd74d8

Reaction equation

NC1CCCOc2ccccc21
5-amino-2,3,4,5-tetrahydro-1-benzoxepine
O=C(Cl)CCCCl
4-chlorobutyryl choride
O=C(CCCCl)NC1CCCOc2ccccc21
5-(4-chlorobutyrylamino)-2,3,4,5-tetrahydro-1-benzoxepine

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    Otherto produce the above compound in the same way as Reference Example 8

Procedure

5-amino-2,3,4,5-tetrahydro-1-benzoxepine and 4-chlorobutyryl choride were used to produce the above compound in the same way as Reference Example 8.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05723475uspto-grants-1998_03