Reaction #1006009
ord-95e3a924d2b44626be2625145913e66b
Reaction equation
(4-(tert-butyl)phenyl)methanamine
ethyl 6-bromoimidazo[1,2-a]pyridine-2-carboxylate
→
title compound
6-Bromo-N-(4-(tert-butyl)benzyl)imidazo[1,2-a]pyridine-2-carboxamide
Reactants
Reagents
None
Conditions
Detailed conditions
See reaction.notes.procedure_details.
Procedure
The title compound was prepared by essentially following the same procedures described for Intermediate I, using (4-(tert-butyl)phenyl)methanamine and ethyl 6-bromoimidazo[1,2-a]pyridine-2-carboxylate as starting materials. 1H NMR (400 MHz, CDCl3) δ 9.53 (s, 1H), 8.60 (s, 1H), 8.41 (s, 1H), 7.88 (d, 1H), 7.79 (d, 1H), 7.36 (d, 2H), 7.32 (d, 2H), 4.60 (d, 2H), 1.38 (s, 9H). MS 385.9, 387.9 (M+1)+.