Reaktion #997934

Reaktionsgleichung

benzoyl peroxide

4-methyl-benzenesulfonyl chloride

N-bromosuccinimide

→

title compound

4-bromomethyl-benzenesulfonyl chloride

Lösungsmittel

1,2-dichloropropane

Reaktionsbedingungen

Aufarbeitung

1. 1
   EinengenThe reaction mixture was concentrated

Vorschrift

At 20° C. benzoyl peroxide (600 mg) was added to a suspension of 4-methyl-benzenesulfonyl chloride (9.5 g) and N-bromosuccinimide (8.9 g) in 1,2-dichloropropane (60 ml). The reaction mixture was stirred at 80° C. for 2 h. The reaction mixture was concentrated and the title compound was obtained as a white solid after recrystallization from heptane. Yield: 2.26 g.

Quelle