Reaktion #997422

ord-dc02bf4d959f4d14877fbcdff952d765

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigehad been produced in Referential Example 28

Vorschrift

The procedure of Referential Example 6 was repeated, except that 1-[4-(6 fluoroimidazo[1,2-a]pyridin-2-yl)phenyl]-1-ethanone (410 mg), which had been produced in Referential Example 28 was used, to thereby yield (E)-3-(dimethylamino)-1-[4-(6-fluoroimidazo[1,2-a]pyridin-2-yl)phenyl]-2-propen-1-one (120 mg). Subsequently, The procedure of Referential Example 3 was repeated, to thereby yield the title compound (75 mg).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08022075B2uspto-grants-2011_09