Reaktion #992694

Reaktionsgleichung

Glycolic acid

Guanidine carbonate

carbon dioxide

→

Guanidinium Glycolate

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe water was removed in vacuo
2. 2
   Temperaturwith heating to approximately 90° C
3. 3
   SonstigeThe product was isolated as a white solid

Vorschrift

Glycolic acid (3.0 g, 39.45 mmol) was dissolved in 15 ml of distilled water. Guanidine carbonate (3.55 g, 19.72 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 4 hours. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as a white solid.

Quelle