Reaktion #992687

Reaktionsgleichung

Tetrafluorosuccinic acid

Guanidine carbonate

carbon dioxide

→

Bis(guanidinium) Tetrafluorosuccinate

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe water was removed in vacuo
2. 2
   Temperaturwith heating to approximately 90° C. for 4 hours
3. 3
   SonstigeThe product was isolated as a white solid

Vorschrift

Tetrafluorosuccinic acid (500 mg, 2.63 mmol) was dissolved in 10 ml of distilled water. Guanidine carbonate (474 mg, 2.63 mmol) was added at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 2 hours. The water was removed in vacuo with heating to approximately 90° C. for 4 hours. The product was isolated as a white solid.

Quelle