Reaktion #992686

Reaktionsgleichung

3,5-Diamino-1,2,4-triazole

Trifluoroacetic acid

→

3,5-Diamino-1,2,4-Triazolium TFA

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe water was removed in vacuo
2. 2
   Temperaturwith heating to approximately 90° C. for 4 hours

Vorschrift

3,5-Diamino-1,2,4-triazole (1.50 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

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