Reaktion #992685

ord-beb52579d6ce409d896a137819b31dd2

Reaktionsgleichung

Nn1cnnc1
4-Amino-1,2,4-triazole
O=C(O)C(F)(F)F
Trifluoroacetic acid
Nn1cn[nH+]c1.O=C([O-])C(F)(F)F
4-Amino-1,2,4-Triazolium TFA

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThe water was removed in vacuo
  2. 2
    Temperaturwith heating to approximately 90° C. for 4 hours

Vorschrift

4-Amino-1,2,4-triazole (1.27 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08012277B2uspto-grants-2011_09