Reaktion #992684
ord-3a9a307eedd64cadac6b3a76c08aacde
Reaktionsgleichung
3-Amino-1,2,4-triazole
Trifluoroacetic acid
→
3-Amino-1,2,4-Triazolium TFA
Reagenzien
Keine
Lösungsmittel
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1SonstigeThe water was removed in vacuo
- 2Temperaturwith heating to approximately 90° C. for 4 hours
Vorschrift
3-Amino-1,2,4-triazole (1.27 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.