Reaktion #992678

ord-ba1587027e5a4b529cc6c14f52331b72

Reaktionsgleichung

CC#N
acetonitrile
Cl.N=C(NN)NN
diaminoguanidine hydrochloride
O=C([O-])C(F)(F)F.[Na+]
sodium trifluoroacetate
→
NC(N)=[N+](N)N.O=C([O-])C(F)(F)F
Diaminoguanidinium trifluoroacetate
[Cl-].[Na+]
Sodium chloride

Edukte

CC#N
acetonitrile
Cl.N=C(NN)NN
diaminoguanidine hydrochloride
O=C([O-])C(F)(F)F.[Na+]
sodium trifluoroacetate

Reagenzien

Keine

Lösungsmittel

CC(C)=O
acetone

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Diaminoguanidinium trifluoroacetate is synthesized by reacting diaminoguanidine hydrochloride and sodium trifluoroacetate in acetone or acetonitrile. Sodium chloride is produced as a byproduct of the reaction and is removed, producing the diaminoguanidinium trifluoroacetate.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08012277B2uspto-grants-2011_09