Reaktion #992677

ord-52e61f1e768a412fb85dfdb976387cab

Reaktionsgleichung

Cl.NC(N)=[N+](N)N
Diaminoguanidinium hydrochloride
NC(N)=O
urea
NC(N)=O.NC(N)=[N+](N)N
Diaminoguanidinium Urea

Reaktionsbedingungen

Temperatur
10°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    workup.STIRRINGstirred until a melt
  2. 2
    Sonstigewas formed, at which time the mixture
  3. 3
    Temperaturwas cooled to room temperature
  4. 4
    Sonstigethe product collected as a white solid

Vorschrift

Diaminoguanidinium hydrochloride (13.0 g, 103.5 mmol) and urea (12.4 g, 207.1 mmol) were placed in a flask with stirring. The flask was heated to 10° C. and stirred until a melt was formed, at which time the mixture was cooled to room temperature and the product collected as a white solid.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08012277B2uspto-grants-2011_09