Reaktion #992677
ord-52e61f1e768a412fb85dfdb976387cab
Reaktionsgleichung
Diaminoguanidinium hydrochloride
urea
→
Diaminoguanidinium Urea
Reagenzien
Keine
Reaktionsbedingungen
Temperatur
10°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1workup.STIRRINGstirred until a melt
- 2Sonstigewas formed, at which time the mixture
- 3Temperaturwas cooled to room temperature
- 4Sonstigethe product collected as a white solid
Vorschrift
Diaminoguanidinium hydrochloride (13.0 g, 103.5 mmol) and urea (12.4 g, 207.1 mmol) were placed in a flask with stirring. The flask was heated to 10° C. and stirred until a melt was formed, at which time the mixture was cooled to room temperature and the product collected as a white solid.