Reaktion #991239

ord-6bc3d61f74cc46fc879b3a8c9515d2cf

Reaktionsgleichung

CCCCCCCCOc1ccc(C(=O)O)cc1
p-octyloxy benzoic acid
BrBr
bromine
CCCCCCCCOc1ccc(C(=O)O)cc1Br
4-octyloxy-3-bromo-benzoic acid

Reagenzien

Keine

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigeis brought to between 50° C. and 55° C.

Vorschrift

37.5 g (0.15 mole) of p-octyloxy benzoic acid are put in suspension in 108 ml of deionized water. The temperature of the reaction medium is brought to between 50° C. and 55° C. and 8.7 ml (0.17 mole) of bromine are added at this temperature over a period of 7 hours 30 minutes.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04230596uspto-grants-1980_10