Reaktion #991109

Reaktionsgleichung

2-ethylhexylamine

methyl crotonate

→

N-(2-ethylhexyl)-crotonamide

Ausbeute 72.1%

Lösungsmittel

n-hexane

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturrefluxed for 6 hours
2. 2
   Waschenwashed first with diluted hydrochloric acid
3. 3
   Trocknenwith 10% sodium hydroxide solution, and subsequently dried with sodium sulfate
4. 4
   SonstigeThe residue was recrystallized from n-hexane

Vorschrift

In a flask, 2.6 g (0.02 mol) of 2-ethylhexylamine and 1.0 g (0.01 mol) of methyl crotonate were admitted and refluxed for 6 hours. The reaction mixture was dissolved in n-hexane, washed first with diluted hydrochloric acid and then with 10% sodium hydroxide solution, and subsequently dried with sodium sulfate. The residue was recrystallized from n-hexane, obtaining 1.42 g of N-(2-ethylhexyl)-crotonamide (yield: 72.1%). Usual analysis was carried out to identify the compound. The results are shown below.

Quelle