Reaktion #985245

ord-2770af4c3d4f4844962ba4d053214fb5

Reaktionsgleichung

[Ca]
calcium
O=P([O-])([O-])[O-]
phosphate
[Na+].[OH-]
NaOH
→
O=P([O-])([O-])[O-].O=P([O-])([O-])[O-].[Ca+2].[Ca+2].[Ca+2]
Calcium Phosphate

Edukte

[Ca]
calcium
O=P([O-])([O-])[O-]
phosphate
[Na+].[OH-]
NaOH

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    workup.ADDITIONto mixing
  2. 2
    SonstigeThe initial solid phase formed immediately
  3. 3
    workup.ADDITIONon mixing
  4. 4
    Filtrationwas filtered
  5. 5
    Waschenwashed (with distilled water+NaOH, pH 10)
  6. 6
    Sonstigefreeze-dried

Vorschrift

The calcium solution was added rapidly with stirring to the phosphate solution. All solutions were adjusted to pH 10 with concentrated NaOH prior to mixing. The initial solid phase formed immediately on mixing was filtered, washed (with distilled water+NaOH, pH 10), and then freeze-dried.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07351280B2uspto-grants-2008_04