Reaktion #969911

ord-c6ab91deaad240dfb3c876796a7b3b5c

Reaktionsgleichung

Nc1ccc(N2CCN3CCC2CC3)cc1
4-(1,4-diaza-bicyclo[3.2.2]non-4-yl)-phenylamine
O=C(Cl)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoyl chloride
→
Cl.O=C(Nc1ccc(N2CCN3CCC2CC3)cc1)c1ccc([N+](=O)[O-])cc1
N-[4-(1,4-Diaza-bicyclo[3.2.2]non-4-yl)-phenyl]-4-nitro-benzamide hydrochloric acid salt

Edukte

Nc1ccc(N2CCN3CCC2CC3)cc1
4-(1,4-diaza-bicyclo[3.2.2]non-4-yl)-phenylamine
O=C(Cl)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoyl chloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Was prepared by Method G from 4-(1,4-diaza-bicyclo[3.2.2]non-4-yl)-phenylamine and 4-nitrobenzoyl chloride. Mp. >280° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08236793B2uspto-grants-2012_08