Reaktion #969910

ord-736219bf5b494695bd967aeae8c13722

Reaktionsgleichung

Nc1ccc(N2CCN3CCC2CC3)cc1
4-(1,4-Diaza-bicyclo[3.2.2]non-4-yl)-phenylamine
O=C(Cl)c1cccc([N+](=O)[O-])c1
3-nitrobenzoyl chloride
→
Cl.O=C(Nc1ccc(N2CCN3CCC2CC3)cc1)c1cccc([N+](=O)[O-])c1
N-[4-(1,4-Diaza-bicyclo[3.2.2]non-4-yl)-phenyl]-3-nitro-benzamide hydrochloric acid salt

Edukte

Nc1ccc(N2CCN3CCC2CC3)cc1
4-(1,4-Diaza-bicyclo[3.2.2]non-4-yl)-phenylamine
O=C(Cl)c1cccc([N+](=O)[O-])c1
3-nitrobenzoyl chloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Was prepared by Method G from 4-(1,4-Diaza-bicyclo[3.2.2]non-4-yl)-phenylamine and 3-nitrobenzoyl chloride. Mp. >280° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08236793B2uspto-grants-2012_08