Reaktion #969907

Reaktionsgleichung

4-(4-nitro-phenyl)-1,4-diaza-bicyclo[3.2.2]nonane

→

4-(1,4-Diaza-bicyclo[3.2.2]non-4-yl)-phenylamine

Lösungsmittel

methanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe crude mixture was filtered through celite
2. 2
   Sonstigethe product was isolated as an oil in quantitative yield

Vorschrift

A mixture of 4-(4-nitro-phenyl)-1,4-diaza-bicyclo[3.2.2]nonane (0.50 g, 2.0 mmol), palladium on carbon (100 mg, 10%) and methanol (60 ml) was stirred for 15 minutes under hydrogen (130 ml of hydrogen was consumed). The crude mixture was filtered through celite and the product was isolated as an oil in quantitative yield.

Quelle