Reaktion #953560

Reaktionsgleichung

4-cyanophenoxy phenyl methane

hydrogen peroxide

NaOH

→

4-Aminocarbonylphenoxy-phenyl methane

Lösungsmittel

ethanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturwas maintained at 40°-50° for 3 hrs
2. 2
   Temperatur, cooled
3. 3
   FiltrationThe product was filtered off
4. 4
   Sonstigerecrystallised from ethanol M.p. 186°-7°

Vorschrift

A mixture of 4-cyanophenoxy phenyl methane (10.45g.; 0.05 mole), 30% hydrogen peroxide (20ml) and 6N NaOH (20ml) and ethanol (30ml) was maintained at 40°-50° for 3 hrs., cooled and neutralised. The product was filtered off and recrystallised from ethanol M.p. 186°-7°.

Quelle