Reaktion #95280

ord-e75f79d7e1024f1bb1cd18596d77bbf9

Reaktionsgleichung

CCCCCC(O)/C=C/I
1-iodo-trans-1-octen-3-ol
BrC(c1ccccc1)(c1ccccc1)c1ccccc1
triphenylmethyl bromide
→
CCCCCC(/C=C/I)OC(c1ccccc1)(c1ccccc1)c1ccccc1
1-iodo-3-triphenylmethoxy-trans-1-octene

Edukte

CCCCCC(O)/C=C/I
1-iodo-trans-1-octen-3-ol
BrC(c1ccccc1)(c1ccccc1)c1ccccc1
triphenylmethyl bromide
—
colorless oil

Reagenzien

Keine

Lösungsmittel

c1ccncc1
pyridine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigegave 13.448 g

Vorschrift

Treatment of 7.62 g. (0.03 mole) of 1-iodo-trans-1-octen-3-ol with 10.67 g. (0.033 mole) of triphenylmethyl bromide in pyridine in the manner described in Example 728 gave 13.448 g. (90%) of a colorless oil.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04343949uspto-grants-1982_08