Reaktion #95279

ord-fe977b0fce07433485951a2064330411

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigegave 58 g
  2. 2
    SonstigeThe oil is purified by adsorption chromatography on a magnesia silica gel column
  3. 3
    Sonstigeto give a light yellow oil

Vorschrift

Treatment of 63 g. (0.25 mole) of 1-iodo-trans-1-octen-3-one (Example 724) with sodium borohydride in the manner described in Example 726 gave 58 g. of yellow oil. The oil is purified by adsorption chromatography on a magnesia silica gel column using benzene as eluent to give a light yellow oil.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04343949uspto-grants-1982_08