Reaktion #94899

ord-e4f5ef47918d4acabaa25bcfb67f94e6

Reaktionsgleichung

CCOC(=O)Cl
ethyl chloroformate
O=C(O)C=C(c1ccccc1)c1cccc([N+](=O)[O-])c1
3-phenyl-3-(3-nitrophenyl)propenoic acid
CCCCCCCCCC(C)N
1-methyldecylamine
→
CCCCCCCCCC(C)NC(=O)C=C(c1ccccc1)c1cccc([N+](=O)[O-])c1
title compound
CCCCCCCCCC(C)NC(=O)C=C(c1ccccc1)c1cccc([N+](=O)[O-])c1
N-(1-Methyldecyl)-3-phenyl-3-(3-nitrophenyl)propenamide

Edukte

CCOC(=O)Cl
ethyl chloroformate
O=C(O)C=C(c1ccccc1)c1cccc([N+](=O)[O-])c1
3-phenyl-3-(3-nitrophenyl)propenoic acid
CCCCCCCCCC(C)N
1-methyldecylamine
—
anhydride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigesubstantially according to the procedure of Preparation 21

Vorschrift

The title compound was prepared from 3-phenyl-3-(3-nitrophenyl)propenoic acid via mixed anhydride formation using ethyl chloroformate, followed by reaction with 1-methyldecylamine, substantially according to the procedure of Preparation 21. This gave a 92% yield of an oil.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04342781uspto-grants-1982_08