Reaktion #94489

ord-00d1da21a3b84804a1208401655501a7

Reaktionsgleichung

NC1CC1
Cyclopropylamine
O=S(=O)(C=Cc1c(Cl)cccc1Cl)N=C([O-])CCl
N-(2,6-dichlorostyrylsulfonyl)chloroacetimidate
→
CC(=NS(=O)(=O)C=Cc1c(Cl)cccc1Cl)NC1CC1
N-cyclopropyl-N'-(2,6-dichlorostyrylsulfonyl) acetamidine

Edukte

NC1CC1
Cyclopropylamine
O=S(=O)(C=Cc1c(Cl)cccc1Cl)N=C([O-])CCl
N-(2,6-dichlorostyrylsulfonyl)chloroacetimidate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Reaction of Cyclopropylamine with N-(2,6-dichlorostyrylsulfonyl)chloroacetimidate according to the procedure of Example 32(b) affords N-cyclopropyl-N'-(2,6-dichlorostyrylsulfonyl) acetamidine, m.p. 121°-124° C. when crystallized from benzene.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04130663uspto-grants-1978_12