Reaktion #939122

Reaktionsgleichung

1,1′carbonyl diimidazole

phenylbutyl alcohol

perhydropyridazine

→

4-phenylbutyl perhydropyridazine-carboxylate

Lösungsmittel

CH2Cl2

CH2Cl2

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONthis solution was then added slowly to a solution
2. 2
   workup.STIRRINGto stir for overnight
3. 3
   EinengenThe crude mixture was then concentrated
4. 4
   Sonstigeused without further purification

Vorschrift

A solution containing 1,1′carbonyl diimidazole (0.893 g, 5.5 mmol) in 5 ml CH2Cl2 was added slowly to a solution of CH2Cl2 containing phenylbutyl alcohol (0.89 ml, 5.77 mmol). After stirring at room temperature for 1 hour, this solution was then added slowly to a solution containing perhydropyridazine mentioned above. The reaction was allowed to stir for overnight. The crude mixture was then concentrated and used without further purification.

Quelle