Reaktion #936271

ord-89bcc112ee1949f392bc459e3e029417

Reaktionsgleichung

COC(=O)C1CCCCC1=O
2-carbomethoxycyclohexanone
BrCCC1OCCCO1
2-(2-bromoethyl)-1,3-dioxane
O=C([O-])[O-].[K+].[K+]
potassium carbonate
→
COC(=O)C1(CCC2OCCCO2)CCCCC1=O
title compound
COC(=O)C1(CCC2OCCCO2)CCCCC1=O
methyl 1-[2-(1,3-dioxan-2-yl)ethyl]-2-oxocyclohexanecarboxylate

Edukte

COC(=O)C1CCCCC1=O
2-carbomethoxycyclohexanone
BrCCC1OCCCO1
2-(2-bromoethyl)-1,3-dioxane
O=C([O-])[O-].[K+].[K+]
potassium carbonate

Reagenzien

Keine

Lösungsmittel

CN(C)C=O
DMF

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

A solution of 2-carbomethoxycyclohexanone in DMF is reacted with 2-(2-bromoethyl)-1,3-dioxane and potassium carbonate by the method of Example 102 to generate the title compound.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06011028uspto-grants-2000_01