Reaktion #936236

ord-3c052107faca43dc997e39c5808c3f29

Reaktionsgleichung

COC1=NC(Cc2ccco2)CCCC1
title product
COC1=NC(Cc2ccco2)CCCC1
2-[(2-furanyl)methyl]-3,4,5,6-tetrahydro-7-methoxy-2H-azepine
[Cl-].[NH4+]
ammonium chloride
→
Cl.N=C1CCCCC(Cc2ccco2)N1
7-[(2-furanyl)methyl]hexahydro-2H-azepin-2-imine, monohydrochloride

Edukte

—
title material
COC1=NC(Cc2ccco2)CCCC1
title product
COC1=NC(Cc2ccco2)CCCC1
2-[(2-furanyl)methyl]-3,4,5,6-tetrahydro-7-methoxy-2H-azepine
[Cl-].[NH4+]
ammonium chloride

Reagenzien

Keine

Lösungsmittel

CO
MeOH

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title product of Example 48 in MeOH is reacted with ammonium chloride by the method of Example 5 to generate the title material.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06011028uspto-grants-2000_01