Reaktion #9346

Reaktionsgleichung

Sodium propanoate

2,6-dipropylphenol

→

phenol

2,6-dipropyl-4-propionylphenol

Lösungsmittel

Triflic Acid

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe resulting waxy solid was purified by chromatography on silica gel

Vorschrift

Sodium propanoate (0.88 g, 1.5 eq) and 2,6-dipropylphenol (1.09 g, 1.0 eq) were combined in Triflic Acid (5.0 g) as in Example 13, step 1. The resulting waxy solid was purified by chromatography on silica gel using ethyl acetate:hexanes:acetic acid (10:90:1) to give the titled phenol.

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