Reaktion #933751

ord-f6610b4e843a46cfb17890cead96a842

Reaktionsgleichung

CCCCCCCCOc1ccc(C(=O)O)cc1
4-octyloxy benzoic acid
CCCCCCBr
bromohexane
CCCCCCOc1ccc(C(=O)O)cc1
4-hexyloxy benzoic acid

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The same procedure as in the synthesis of 4-octyloxy benzoic acid of Example 26 was repeated except that bromohexane was used instead of bromooctane to obtain 4-hexyloxy benzoic acid. This 4-hexyloxy benzoic acid was condensed with (+)-4-(2-methyloctanoyl) phenol in the same manner as in the synthesis of 4-(2-methyloctanoyl) phenyl, 4-octyloxy benzoic acid ester of Example 26 to synthesize 4-(2-methyloctanoyl) phenyl, 4-hexyloxy benzoic acid ester having the aforementioned physical and chemical properties.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05137653uspto-grants-1992_08