Reaktion #928060

Reaktionsgleichung

8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one

N-(3-trifluoromethylphenyl)-4-aminobenzenesulfonamide

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title compound

Ausbeute 29.0%

4-[(7-Oxo-6,7-dihydro-1-thia-3,6-diaza-as-indacen-8-ylidenemethyl)-amino]-N-(3-trifluoromethyl-phenyl)-benzenesulfonamide

Ausbeute 29.0%

Reaktionsbedingungen

Vorschrift

The title compound was prepared in 29% yield from 8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one and N-(3-trifluoromethylphenyl)-4-aminobenzenesulfonamide according to Procedure J: 1H NMR (DMSO-d6): δ11.2 (d, 1H), 10.9 (s, 1H), 10.7 (s, 1H), 9.3 (s, 1H), 8.1 (d, 1H), 7.8 (m, 3H), 7.5 (m, 4H), 7.1 (d, 1H); APCI−MS m/z 515 (M−H)−.

Quelle