Reaktion #927213

Reaktionsgleichung

methyl 6-hydroxy-2naphthyl-α-methylacetate

methylacetate

chlorodimethyl ether

→

methyl 6-methoxymethyloxy-2-naphthyl-α-methylacetate

Lösungsmittel

dimethylformamide

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONA mixture of 23 g
2. 2
   SonstigeThe reaction mixture is evaporated under reduced pressure

Vorschrift

A mixture of 23 g. of methyl 6-hydroxy-2naphthyl-α-methylacetate, methylacetate, 25 g. of chlorodimethyl ether, and 500 ml. of dimethylformamide is allowed to stand at room temperature for 12 hours. The reaction mixture is evaporated under reduced pressure to give methyl 6-methoxymethyloxy-2-naphthyl-α-methylacetate.

Quelle