Reaktion #926953

ord-40c9389efb9947079670005e1abec092

Reaktionsgleichung

C=CCCC(C)Cl
5-chloro-1-hexene
CCCCCCCCCCCCCCCCC1CO1
1,2-epoxy octadecane
CC(C)(C)OOC(=O)C(C)(C)C
t-butyl peroxypivalate
CC1=CC(=O)OC1=O
methylmaleic anhydride
O=C1C=C(Cl)C(=O)O1
chloromaleic anhydride
C=CCCCCCCCCCCCCCCCC
1-octadecene
C=Cc1ccccc1
styrene
CCCC1OC1(C)c1ccccc1
2,3 -epoxy-2-phenylhexane

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeIn like manner a thickened, moldable intermediate is produced when appropriate amounts

Vorschrift

In like manner a thickened, moldable intermediate is produced when appropriate amounts, as described herein, of 5-chloro-1-hexene, methylmaleic anhydride, a 1,2-epoxy octadecane, a 4:1 styrene-maleic anhydride copolymer and pyridine are heated to about 45° C. in the presence of t-butyl peroxypivalate. Also a thickened, moldable intermediate is produced when appropriate amounts of 1-octadecene, styrene, chloromaleic anhydride, 2,3 -epoxy-2-phenylhexane, a 1-hexene-maleic anhydride copolymer and N-methylpiperazine are heated to about 45° C. in the presence of 2-t-butylazo-2-cyano-4-methoxy-4-methylpentane.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04097449uspto-grants-1978_06