Reaktion #92497

Reaktionsgleichung

Compound 7p

3-(4-(3,4-dichlorophenyl)piperazine-1-yl)propan-1-ol

triphenylphosphine resin

imidazole

iodine

→

1-(3,4-dichlorophenyl)-4-(3-iodopropyl)piperazine

Lösungsmittel

DCM

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe product compound 11p was used without further purification for the next reaction

Vorschrift

Compound 7p was mixed with triphenylphosphine resin, imidazole and iodine in DCM as described in General Procedure B. The product compound 11p was used without further purification for the next reaction. MS (LC/MS, ESI): 399 (M+H).

Quelle