Reaktion #9099

Reaktionsgleichung

acetyl chloride

piperidine

2-chlorobenzaldehyde

→

1-(2-chloro-benzylidene)-piperidinium chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigewith general synthesis instructions 3

Vorschrift

The reaction of 8.5 g (0.100 mol) piperidine and 7.0 g (0.050 mol) 2-chlorobenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 3.9 g (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 7.1 g (corresponding to 58% of the yield calculated by theory) 1-(2-chloro-benzylidene)-piperidinium chloride.

Quelle