Reaktion #9077

ord-72da6cfad289430d96716ceae4346d94

Reaktionsgleichung

CCOC(=O)c1cc2ccccc2[nH]1
1H-indole-2-carboxylic acid ethyl ester
C[N+](C)=Cc1ccccc1.[Cl-]
benzylidene-dimethyl-ammonium chloride
→
CCOC(=O)c1[nH]c2ccccc2c1C(c1ccccc1)N(C)C
3-(Dimethylaminophenylmethyl)-1H-indole-2-carboxylic Acid Ethyl Ester

Edukte

CCOC(=O)c1cc2ccccc2[nH]1
1H-indole-2-carboxylic acid ethyl ester
C[N+](C)=Cc1ccccc1.[Cl-]
benzylidene-dimethyl-ammonium chloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The preparation was carried out in accordance with general synthesis instructions 4 from 1H-indole-2-carboxylic acid ethyl ester and benzylidene-dimethyl-ammonium chloride. For characterization, an ESI-MS was recorded:

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07091220B2uspto-grants-2006_08