Reaktion #878

ord-59691e7705044240a0b61a8537732528

Reaktionsgleichung

O=P([O-])([O-])[O-].[Na+].[Na+].[Na+]
sodium phosphate
[Ca+2].[Cl-].[Cl-]
calcium chloride
→
O=P([O-])([O-])[O-].O=P([O-])([O-])[O-].[Ca+2].[Ca+2].[Ca+2]
tricalcium phosphate

Edukte

O=P([O-])([O-])[O-].[Na+].[Na+].[Na+]
sodium phosphate
[Ca+2].[Cl-].[Cl-]
calcium chloride

Reagenzien

Keine

Lösungsmittel

O
water
O
Solution A
O
water
O
water
O
Solution B
O
water
O
water

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

39.3 Grams of sodium phosphate were dissolved in 150 grams of water (Solution A). In a separate beaker, 22.65 grams of calcium chloride were dissolved in 150 grams of water (Solution B). Each of the above solutions were added simultaneously to 200 grams of water, while being sheared at speeds of 12,000 rpm. This shearing was necessary since the viscosity resulting from the in situ formation of tricalcium phosphate (TCP) particulates needs to be broken down into submicron size in order to be effective as a stabilizer. The amount of in situ TCP generated in this case was 16.0 grams.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05723252uspto-grants-1998_03