Reaktion #87652

Reaktionsgleichung

4-fluoro-3-(trifluoromethyl)aniline

NaNO2

SnCl2.2H2O

→

desired product

1-(4-fluoro-3-(trifluoromethyl)phenyl)hydrazine

Lösungsmittel

HCl

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe title compound was prepared

Vorschrift

The title compound was prepared according to the procedure described in step-1 of Intermediate-61 by using 4-fluoro-3-(trifluoromethyl)aniline (3.0 g, 0.016 mmol), NaNO2 (1.73 g, 0.025 mmol), SnCl2.2H2O (9.39 g, 0.041 mmol) and conc. HCl (100 mL) to afford 2.0 g of the desired product.

Quelle