Reaktion #87648

Reaktionsgleichung

5-((2,2,2-trifluoroacetamido)methyl)-2-chloro-4-methoxybenzoic acid

oxalyl chloride

ammonia

→

desired product

5-((2,2,2-trifluoroacetamido)methyl)-2-chloro-4-methoxybenzamide

Lösungsmittel

THF

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe title compound was prepared

Vorschrift

The title compound was prepared according to the procedure described in step-2 of Intermediate-26 by using 5-((2,2,2-trifluoroacetamido)methyl)-2-chloro-4-methoxybenzoic acid (1.0 g), oxalyl chloride (1.0 mL), THF (50 mL) and ammonia gas to afford 0.800 g of the desired product.

Quelle