Reaktion #875

ord-d6db1ba811484e3384ed2f23fdfc613c

Reaktionsgleichung

O=P([O-])([O-])[O-].[Na+].[Na+].[Na+]
sodium phosphate
[Ca+2].[Cl-].[Cl-]
calcium chloride
O=P([O-])([O-])[O-].O=P([O-])([O-])[O-].[Ca+2].[Ca+2].[Ca+2]
tricalcium phosphate

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

78.6 Grams of sodium phosphate were dissolved in 300 grams of water. In a separate beaker, 45.3 grams of calcium chloride were dissolved in 300 grams of water. 200 Grams of each of the above solutions were added simultaneously to 200 grams of water, while being sheared at speeds of 12,000 rpm. This shearing was accomplished since the viscosity resulting from the in situ formation of tricalcium phosphate (TCP) particulates needs to be broken down into submicron size in order to be more effective as a stabilizer. The amount of in situ TCP generated in this Example was 21.3 grams.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05723252uspto-grants-1998_03