Reaktion #86648

Reaktionsgleichung

Methyl ester

(R)-3-Allylsulfanyl-2-tert-butoxycarbonylamino-propionic acid methyl ester

hydrogen chloride

→

(R)-3-Allylsulfanyl-2-amino-propionic acid methyl ester hydrochloride

Lösungsmittel

1,4-dioxane

Reaktionsbedingungen

Aufarbeitung

1. 1
   Einengenbefore being concentrated in vacuo
2. 2
   Sonstigeto yield a white solid, 2.46 g, 100%

Vorschrift

Methyl ester 29 (3.20 g, 11.6 mmol) was dissolved in 4M hydrogen chloride in 1,4-dioxane (40 mL). The resultant solution was stirred at rt for 18 h before being concentrated in vacuo to yield a white solid, 2.46 g, 100%.

Quelle