Reaktion #86331

Reaktionsgleichung

5-bromopyridine-2-sulfonyl chloride hydrochloride

ammonium hydroxide

→

title compound

5-bromopyridine-2-sulfonamide

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeTo a 4 mL vial equipped with a magnetic stir bar
2. 2
   Sonstigeto give a white suspension, which
3. 3
   SonstigeThe solvent was subsequently evaporated

Vorschrift

To a 4 mL vial equipped with a magnetic stir bar were added 5-bromopyridine-2-sulfonyl chloride hydrochloride (250 mg, 0.853 mmol) and ammonium hydroxide (1329 μL, 34.1 mmol) to give a white suspension, which was heated to 70° C. in a sand bath overnight. The solvent was subsequently evaporated to give the title compound, which was used without further purification.

Quelle