Reaktion #85820

ord-3adef84ce87b4695bba69b0c8b6f8979

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    EinengenThe mixture was concentrated in vacuo

Vorschrift

(R)-tert-butyl 3-ureidopyrrolidine-1-carboxylate from step A was treated with HCl solution (in EtOAc, 30 mL) for 2 hours. The mixture was concentrated in vacuo to give the crude title compound. MS (m/z): 130 (M+H)+.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US09434726B2uspto-grants-2016_09