Reaktion #85803

Reaktionsgleichung

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine

bromoethane

NaH

THF

→

crude title compound

N,N-diethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine

Reaktionsbedingungen

Aufarbeitung

1. 1
   Einengenconcentrated in vacuo

Vorschrift

A mixture of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine (100 mg, 0.45 mmol) and bromoethane (200 mg, 1.8 mmol), NaH (100 mg, 1.8 mmol) in THF was stirred at room temperature overnight, and concentrated in vacuo to give the crude title compound used for the next step. MS (m/z): 276 (M+H)+.

Quelle