Reaktion #85130

ord-586c77b3457b4c84a14357ce1c991451

Reaktionsgleichung

CCOc1cnc(OC)cc1-c1cc(Cl)ccc1C#N
4-chloro-2-(5-ethoxy-2-methoxypyridin-4-yl)benzonitrile
Br.c1cc[nH+]cc1
pyridinium hydrobromide
CCOc1c[nH]c(=O)cc1-c1cc(Cl)ccc1C#N
4-Chloro-2-(5-ethoxy-2-oxo-1,2-dihydropyridin-4-yl)benzonitrile

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

135 mg (0.44 mmol) of 4-chloro-2-(5-ethoxy-2-methoxypyridin-4-yl)benzonitrile and pyridinium hydrobromide were reacted according to General Method 3A. Yield: 134 mg (purity 76%, 83% of theory)

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US09434690B2uspto-grants-2016_09