Reaktion #85006

ord-b2ca3f1fe6934a5da59883a869dc3121

Reaktionsgleichung

COc1cc(-c2cc(Cl)ccc2C#N)c(C(F)F)cn1
4-chloro-2-[5-(difluoromethyl)-2-methoxypyridin-4-yl]benzonitrile
Br.c1cc[nH+]cc1
pyridinium hydrobromide
N#Cc1ccc(Cl)cc1-c1cc(=O)[nH]cc1C(F)F
4-Chloro-2-[5-(difluoromethyl)-2-oxo-1,2-dihydropyridin-4-yl]benzonitrile

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

216 mg (0.73 mmol) of 4-chloro-2-[5-(difluoromethyl)-2-methoxypyridin-4-yl]benzonitrile and pyridinium hydrobromide were reacted according to General Method 3A. Yield: 215 mg (purity 64%, 67% of theory)

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US09434690B2uspto-grants-2016_09