Reaktion #84846

Reaktionsgleichung

2-(4-bromo-3,5-dimethoxyphenyl)furan

2-(4-((dimethylamino)methyl)phenyl)-N,2-dimethoxy-N-methylacetamide

→

1-(5-(4-Bromo-3,5-dimethoxyphenyl)furan-2-yl)-2-(4-((dimethylamino)methyl)phenyl)-2-methoxyethanone

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigePurification by chromatography (4% MeOH/CH2Cl2)

Vorschrift

1-(5-(4-Bromo-3,5-dimethoxyphenyl)furan-2-yl)-2-(4-((dimethylamino)methyl)phenyl)-2-methoxyethanone was prepared from 2-(4-bromo-3,5-dimethoxyphenyl)furan and 2-(4-((dimethylamino)methyl)phenyl)-N,2-dimethoxy-N-methylacetamide according to the procedure used in Example 30. Purification by chromatography (4% MeOH/CH2Cl2) gave the product as a pale yellow oil (0.004 g, 1% yield). MS: ink 488.3 [M+H]+.

Quelle