Reaktion #84544

Reaktionsgleichung

2-(cyclohexyloxy)acetic acid

dichlorosulfane

→

title compound

2-(cyclohexyloxy)acetyl chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturwas refluxed for 2 h
2. 2
   Einengenconcentrated in vacuo

Vorschrift

A mixture of 2-(cyclohexyloxy)acetic acid (0.90 g, 5.69 mmol) and dichlorosulfane (10 mL) was refluxed for 2 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound as yellow oil, which was used for next step without further purification.

Quelle