Reaktion #84428

Reaktionsgleichung

4-(5-nitropyridin-2-yl)morpholine

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title compound

Ausbeute 99.0%

6-morpholinopyridin-3-amine

Ausbeute 99.0%

Lösungsmittel

THF

Reaktionsbedingungen

Aufarbeitung

1. 1
   Filtrationfiltered
2. 2
   EinengenThe filtrate was concentrated in vacuo

Vorschrift

To a solution of 4-(5-nitropyridin-2-yl)morpholine (3.89 g, 18.60 mmol) in THF (100 mL) was added catalyst Pd/C (0.5 g). The reaction was stirred at rt under H2 overnight, and filtered. The filtrate was concentrated in vacuo to give the title compound as a brown-red solid (3.30 g, 99%).

Quelle